How can I extract myristicin from nutmeg oil?
Extracting Myristicin & Safrole from Nutmeg. The shot would be to soxhlet extract the oil from a few kilos of nutmegs, strip the solvent (pref. under vacuum) perhaps filter/press the oil at room temperature to remove the nutmeg fats (myristic acid and glycerides) Then fractionally distill at reduced pressure to obtain the correct fraction.
Why does nutmeg + alcohol equal pure myristicin?
Nutmeg + alcohol does not equal pure myristicin. Myristicin is a non-polar compound, and as such obtaining a high-purity solution of it would require the distillation of nutmeg oil. This isn’t too hard to do in a clandestine lab if you can set up a still, but it takes more work than soaking McCormick’s in alcohol.
Is it safe to extract myristicin?
What that guy was doing doesn't sound safe. However, you can extract myristicin (along with a bunch of other stuff) in a much safer way with a simple solvent extraction.
How do I make myristicin paste?
Now you will have pretty pure myristicin as a yellow paste. Soak the myristicin in windex for 1 hour. Use about half a cup per batch (starting from 15g of herb or around 30g nutmeg). Now filter it out. It should not dissolve in the windex (5% ammonia 95% water and blue coloring). If it does (it never has when ive done this) boil ot off OUTSIDE.
Where is myristicin found in nutmeg?
Myristicin is a naturally-occurring deliriant substance of the phenylpropene class. It is present in small amounts in the essential oil of nutmeg and, to a lesser extent, in other spices such as parsley and dill.
How do you extract oil from nutmeg?
There are two general methods by which the fixed oil of nutmeg is extracted. In one method, sound, ground nutmeg is subjected to intense hydraulic pressure and heat (heated plates in the presence of steam) while, in the other the ground nutmeg is extracted by refluxing with a solvent like diethyl ether.
Does myristicin evaporate?
6,7 Myristicin is a derivative of phenylpropanoid compounds, in the form of a clear liquid, not soluble in water but soluble in organic solvents. It smells like spices, and the aroma is sharp and easily vaporized.
What is extracted from nutmeg?
Fifty-three compounds in the nutmeg oleoresin have been identified to account for >90 % of the total oil content. Sabinene, myristicin, elemicin, α-pinene, β-pinene, limonene, terpinen-4-ol and myristic acid were found as major compounds of all the nutmeg oleoresins obtained by different techniques.
What is nutmeg oil made out of?
Myristica fragransNutmeg Oil is distilled from the seed located in the nutmeg fruit (Myristica fragrans). It is clear or pale yellow in appearance and tastes and smells of nutmeg. It is most commonly used as a flavorant in a baked good, sweets and syrups.
What nutmeg oil is good for?
Brilliant Advantages Of Nutmeg Essential Oil For Overall Wellbeing:Heals Mental Stress.Soothes Menstrual Cramps.Eliminates Mouth Odour.Rectifies Skin Conditions.Treats Respiratory Problems.Rectifies Gut Problems.Boosts Sexual Stamina.Adds Volume To Hair.
Is Myristicin soluble in water?
Insoluble in water, slightly soluble in ethanol, soluble in ether and benzene.
Is nutmeg water soluble?
Nutmeg oil is very sensitive towards light and temperature, very soluble in ethanol but not water soluble [12].
Does nutmeg contain oil?
Nutmeg oil is a volatile essential oil from nutmeg (Myristica fragrans). The oil is colorless or light yellow and smells and tastes of nutmeg. It contains numerous components of interest to the oleochemical industry. The essential oil consists of approximately 90% terpene hydrocarbons.
Is myristicin a poisonous compound?
Toxicity. Myristicin has been proven to be cytotoxic, or toxic to living cells.
Is nutmeg shell edible?
the shell is mace, the inside is nutmeg. go easy on it mind, it's poisonous in any quantity (like if you tipped a whole jar in something by mistake).
What part of nutmeg are we eating?
When fully mature it splits in two, exposing a crimson-coloured aril, the mace, surrounding a single shiny brown seed, the nutmeg. The pulp of the fruit is eaten locally.
Why do people use nutmeg?
Indigenous peoples have used nutmeg for centuries to treat illness of the stomach and kidneys, as well as just about everything else. (1) Nutmeg also has a long, relatively speaking of course, history as a hallucinogen. Many (now) prominent peple have published on its psychedelic effects.
Where did nutmeg originate?
Nutmeg by Tlongacre (CC BY-ND 2.0) Nutmeg dates back to Indonesia and the “Spice Islands” near the turn of the 16th century. Then, much of the area was controlled by the Portugese, and in particular, the Banda Islands. At the time, these islands were the sole locale of Myristica fragrans, otherwise known as the nutmeg tree.
What is a nutmeg tree?
At the time, these islands were the sole locale of Myristica fragrans, otherwise known as the nutmeg tree . The nutmeg tree is a 10 meter, bushy, evergreen that grows best in wet, tropic locations. Its fruit will split open, revealing a brown seed covered with a bright red lattice.
How old was the first person to die from eating nutmeg?
The first occurred (date unknown) in an 8 year old boy who ate two nutmegs and became comatose (10). He died 24 hours later, and the symptoms were reported as similar to that of opium. The second is a 55 year old male that presented with nutmeg in the stomach contents at autopsy (11).
Is myristicin a toxic drug?
The most common symptoms were tachycardia, vomiting, agitation, and hallucinations. Good times, good times. So despite being relatively non-toxic, it always depends upon the dose and the person. And if myristicin really is being metabolized to MMDA, then liver function and other foods and drugs on board will play a role.
Can you take nutmeg for a trip?
In search of a psychedelic high, some teenager, somewhere, will turn to nutmeg. Yes, that aromatic spice used in pumpkin pie and eggnog can take you for a trip. And people have been trippin’ on nutmeg for centuries.
Who is the godfather of hallucinogens?
This includes Dr. Andrew Weil, he of healthy living fame (2), Albert Hofmann of LSD fame (3), and Alexander Shulgin, the “Godfather” of synthetic hallucinogens and PiHKAL fame (4).
How to make myristicin paste?
Now you will have pretty pure myristicin as a yellow paste. Soak the myristicin in windex for 1 hour. Use about half a cup per batch (starting from 15g of herb or around 30g nutmeg). Now filter it out.
How to make a MMDA?
You can either start from parsley, cilantro, or nutmeg. Heat up some alcohol (vodka or everclear) in the microwave for about 30 seconds (I would use 4 shots per small McCormick bottle of nutmeg or 15g of fresh cilantro or parsley. Put your herb in it. Stirr good let sit for an hour. Come back to stirr it again after 30 minutes, then again after 55 minutes. Now filter it. Boil off the alcohol at 200F (212F if its not everclear). Now you will have pretty pure myristicin as a yellow paste. Soak the myristicin in windex for 1 hour. Use about half a cup per batch (starting from 15g of herb or around 30g nutmeg). Now filter it out. It should not dissolve in the windex (5% ammonia 95% water and blue coloring). If it does (it never has when ive done this) boil ot off OUTSIDE. Now you have almost 100% pure MMDA minus very small amounts of other plant materials. You can also wash it with acetone to obtain fully pure MMDA.
